論文

査読有り
2011年12月

Nondestructive high-resolution solid-state NMR of rotating thin films at the magic-angle

JOURNAL OF MAGNETIC RESONANCE
  • Munehiro Inukai
  • ,
  • Yasuto Noda
  • ,
  • Kazuyuki Takeda

213
1
開始ページ
192
終了ページ
195
記述言語
英語
掲載種別
研究論文(学術雑誌)
DOI
10.1016/j.jmr.2011.09.013
出版者・発行元
ACADEMIC PRESS INC ELSEVIER SCIENCE

We present a new approach to nondestructive magic-angle spinning (MAS) nuclear magnetic resonance (NMR) for thin films. In this scheme, the sample put on the top of a rotor is spun using the conventional MAS system, and the NMR signals are detected with an additional coil. Stable spinning of disk-shaped samples with diameters of 7 mm and 12 mm at 14.2 and 7 kHz are feasible. We present Li-7 MAS NMR experiments of a thin-film sample of LiCoO2 with a thickness of 200 nm. Taking advantage of the nondestructive feature of the experiment, we also demonstrate ex situ experiments, by tracing conformation change upon annealing for various durations. This approach opens the door for in situ MAS NMR of thin-film devices as well. (C) 2011 Elsevier Inc. All rights reserved.

Web of Science ® 被引用回数 : 4

リンク情報
DOI
https://doi.org/10.1016/j.jmr.2011.09.013
CiNii Articles
http://ci.nii.ac.jp/naid/120003534360
PubMed
https://www.ncbi.nlm.nih.gov/pubmed/21958755
Web of Science
https://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=JSTA_CEL&SrcApp=J_Gate_JST&DestLinkType=FullRecord&KeyUT=WOS:000296997800026&DestApp=WOS_CPL
URL
http://www.scopus.com/inward/record.url?eid=2-s2.0-80055086024&partnerID=MN8TOARS
URL
http://orcid.org/0000-0003-4830-6888

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