2021年
Iron nitride, α″-Fe<inf>16</inf>N<inf>2</inf>, around <100> interstitial type dislocation loops in neutron-irradiated iron
Philosophical Magazine
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- 巻
- 101
- 号
- 10
- 開始ページ
- 1202
- 終了ページ
- 1213
- 記述言語
- 掲載種別
- 研究論文(学術雑誌)
- DOI
- 10.1080/14786435.2021.1891317
Atom probe tomography (APT) and selected area electron diffraction (SAED) by transmission electron microscopy (TEM) were applied to nano-scale precipitates formed in a neutron-irradiated iron (99.99% pure) at high temperatures. In the conventional TEM, we discovered donut-type precipitates on the {100} planes that formed at the dilatational side of interstitial type dislocation loops with the Burgers vector of <100> on the habit planes of {100} in the bcc iron lattice. The precipitates were identified as nitride, bct α″-Fe N , by chemical composition and lattice structural analyses using APT and SAED. Image contrasts of the α″-Fe N in a weak beam dark-field electron microscopy study were carefully analysed with the diffraction vector and the sign of deviation parameter from the Bragg condition, and it was concluded to be a selective visualisation of α″-Fe N on one of the {100} planes. These results were in agreement with the crystallographic orientation between the α″-Fe N and matrix iron, thereby bridging a knowledge gap in α″-Fe N formation during neutron irradiation using a sodium-cooled experimental fast reactor, JOYO, or a 14 MeV D-T neutron source, RTNS-II. 16 2 16 2 16 2 16 2 16 2
- リンク情報
- ID情報
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- DOI : 10.1080/14786435.2021.1891317
- ISSN : 1478-6435
- eISSN : 1478-6443
- SCOPUS ID : 85101886282