論文

査読有り 本文へのリンクあり
2021年

Analysis of Nano-hardness Distribution Near the Ferrite-martensite Interface in a Dual Phase Steel with Factorization of Its Scattering Behavior

ISIJ INTERNATIONAL
  • Reon Ando
  • ,
  • Takashi Matsuno
  • ,
  • Tomoko Matsuda
  • ,
  • Norio Yamashita
  • ,
  • Hideo Yokota
  • ,
  • Kenta Goto
  • ,
  • Ikumu Watanabe

61
1
開始ページ
473
終了ページ
480
記述言語
英語
掲載種別
研究論文(学術雑誌)
DOI
10.2355/isijinternational.ISIJINT-2020-546
出版者・発行元
IRON STEEL INST JAPAN KEIDANREN KAIKAN

Herein, we investigated the local preliminary hardening of ferrite near the ferrite-martensite interfaces in a dual-phase (DP) steel. Geometrically necessary dislocations (GNDs), generated due to interfacial misfit between different phases, may cause preliminary hardening of ferrite around such interfaces. However, for nano-hardness distribution, the hardened zone was not evidently detected by scattering measurement. Thus, we factorized nano-hardness scattering to estimate the actual ferrite hardness near ferrite-martensite interfaces.First, nano-hardness was measured around a martensite island using a conical nano-indenter in the DP steel containing 10% martensite by volume. Taking into account the scattering, the nano-hardness measurement converged to the hardness of ferrite, exceeding the distance corresponding to the nano-indenter radius. Thus, a preliminary hardening zone was not detected. Subsequently, the surface of the nano indented microstructure was polished and observed using scanning electron microscopy (SEM) by analyzing electron back scattering diffraction (EBSD). This analysis confirmed the presence of the nano-indented microstructure under ferrite. Moreover, it established that the majority of the irregularly higher nano hardness was caused by the buried martensite under ferrite. The value of the kernel average misorientation (KAM), which is proportional to the GND density for other irregularly higher nano-hardness points, was higher for the nano-indented microstructure as compared to that of the buried martensite. On the other hand, the ferrite was expanded under the nano-indented points for the majority of the irregularly lower nano-hardness, with some exceptions. Further, soft martensite was observed to induce irregularly lower nano-hardness locally around the interface.

リンク情報
DOI
https://doi.org/10.2355/isijinternational.ISIJINT-2020-546 本文へのリンクあり
Web of Science
https://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=JSTA_CEL&SrcApp=J_Gate_JST&DestLinkType=FullRecord&KeyUT=WOS:000630090800054&DestApp=WOS_CPL
Scopus
https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=85100119899&origin=inward 本文へのリンクあり
Scopus Citedby
https://www.scopus.com/inward/citedby.uri?partnerID=HzOxMe3b&scp=85100119899&origin=inward
ID情報
  • DOI : 10.2355/isijinternational.ISIJINT-2020-546
  • ISSN : 0915-1559
  • eISSN : 1347-5460
  • ORCIDのPut Code : 86988573
  • SCOPUS ID : 85100119899
  • Web of Science ID : WOS:000630090800054

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