論文

査読有り
2017年

Porous Ti-Al Intermetallic Based Alloys Fabricated by Pressure-Sintering Elemental Powders with a Space holder Powder

MRS ADVANCES
  • Naoki Takata
  • ,
  • Keisuke Uematsu
  • ,
  • Makoto Kobashi

2
26
開始ページ
1387
終了ページ
1392
記述言語
英語
掲載種別
研究論文(学術雑誌)
DOI
10.1557/adv.2017.123
出版者・発行元
CAMBRIDGE UNIV PRESS

In the present study, we have attempted to produce the porous Ti-Al intermetallic based alloys by pressure-sintering of the elemental powders of Ti and Al through a combustion reaction, with a NaCl space holder to achieve the development of a highly porous structure. The powders of Ti (particle size: <45 pm) and Al (particle size: <45 pm) were mixed to various total compositions of Ti-0-40 Al (at.%), and NaCl (particle size: 300-400 mu m) was mixed with the Ti/Al powder to give a highly porous structure. The mixed powder was sintered at 700 degrees C: under a constant pressure of 30 MPa to form cylindrical specimens with a diameter of 20 mm. The soaking of the specimens in pure water allows for the removal of NaCl (with a volume fraction of 60 %) and the formation of the pores to achieve a controlled relative density of 0.4. The present process can produce porous Ti Al alloys with various compositions. In as-sintered Ti-AI specimens, an inhomogeneous microstructure consisting of Ti particles surrounded by the a Ti Al alloy layer (various Ti-Al intermetallic phases) was observed. The as-sintered specimens exhibited the brittle behavior under compression, which is independent of their Al content. However, in a Ti-20Al alloy heat-treated at 1300 degrees C, a nearly Ti3Al single-phase microstructure appeared in the porous specimen. The heat-treated porous Ti-20Al alloy shows both a high plateau-strength level of approximately 100 MPa and a high plateau-end strain over 50%, resulting in a high absorption energy. The present results demonstrate that controlling the microstructure for the formation of the Ti(3)AI single-phase would he an effective method to achieve high energy absorption capacity of the porous Ti Al alloy.

リンク情報
DOI
https://doi.org/10.1557/adv.2017.123
Web of Science
https://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=JSTA_CEL&SrcApp=J_Gate_JST&DestLinkType=FullRecord&KeyUT=WOS:000412747600004&DestApp=WOS_CPL
ID情報
  • DOI : 10.1557/adv.2017.123
  • ISSN : 2059-8521
  • Web of Science ID : WOS:000412747600004

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