MISC

2008年3月

Fabrication of highly dense MgB2 bulk at ambient pressure

SUPERCONDUCTOR SCIENCE & TECHNOLOGY
  • M. Maeda
  • ,
  • Y. Zhao
  • ,
  • S. X. Dou
  • ,
  • Y. Nakayama
  • ,
  • T. Kawakami
  • ,
  • H. Kobayashi
  • ,
  • Y. Kubota

21
3
開始ページ
1
終了ページ
4
記述言語
英語
掲載種別
DOI
10.1088/0953-2048/21/3/032004
出版者・発行元
IOP PUBLISHING LTD

We report an in situ heat-treatment technique for the preparation of near-fully-dense un-doped MgB2 bulks that also provides very strong in-field pinning. The high density was achieved without using high-pressure apparatus. The heat-treatment of compacted boron sealed in a Ta tube with Mg pellets employs a short high-temperature sintering at 1100 degrees C first, followed by a low-temperature annealing below 660 degrees C. A high density of 2.5 g cm(-3) (95% of the theoretical density) was achieved in the bulks treated by the two-step process. The in-field J(c) is nearly one order of magnitude higher than for the samples prepared by single-step sintering at high or low temperature. Microstructural analysis suggested a unique feature of well-connected small grains with a high level of disorder in the MgB2 samples created by the two-step process.

リンク情報
DOI
https://doi.org/10.1088/0953-2048/21/3/032004
Web of Science
https://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=JSTA_CEL&SrcApp=J_Gate_JST&DestLinkType=FullRecord&KeyUT=WOS:000254407100016&DestApp=WOS_CPL
ID情報
  • DOI : 10.1088/0953-2048/21/3/032004
  • ISSN : 0953-2048
  • Web of Science ID : WOS:000254407100016

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