論文

査読有り
2017年5月

Effect of hydrogenation disproportionation conditions on magnetic anisotropy in Nd-Fe-B powder prepared by dynamic hydrogenation disproportionation desorption recombination

AIP ADVANCES
  • Masao Yamazaki
  • ,
  • Takashi Horikawa
  • ,
  • Chisato Mishima
  • ,
  • Masashi Matsuura
  • ,
  • Nobuki Tezuka
  • ,
  • Satoshi Sugimoto

7
5
開始ページ
056220
終了ページ
記述言語
英語
掲載種別
研究論文(学術雑誌)
DOI
10.1063/1.4975697
出版者・発行元
AMER INST PHYSICS

Various anisotropic Nd-Fe-B magnetic powders were prepared by the dynamic hydrogenation disproportionation desorption recombination (d-HDDR) treatment with different hydrogenation disproportionation (HD) times (tHD). The resulting magnetic properties and microstructural changes were investigated. The magnetic anisotropy was decreased with increasing tHD. In the d-HDDR powders with higher magnetic anisotropy, fine (200-600 nm) and coarse (600-1200 nm) Nd2Fe14B grains were observed. The coarse Nd2Fe14B grains showed highly crystallographic alignment of the c-axis than fine Nd2Fe14B grains. In the highly anisotropic Nd2Fe14B d-HDDR powder, a large area fraction of lamellar-like structures consisting of NdH2 and alpha-Fe were observed after HD treatment. Furthermore, the mean diameter of the lamellar-like regions, where lamellar-like structures orientate to the same direction in the HD-treated alloys was close to that of coarse Nd2Fe14B grains after d-HDDR treatment. Thus, the lamellar-like regions were converted into the crystallographically aligned coarse Nd2Fe14B grains during desorption recombination treatment, and magnetic anisotropy is closely related to the volume fraction of lamellar-like regions observed after HD treatment. (C) 2017 Author(s).

リンク情報
DOI
https://doi.org/10.1063/1.4975697
Web of Science
https://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=JSTA_CEL&SrcApp=J_Gate_JST&DestLinkType=FullRecord&KeyUT=WOS:000402797100220&DestApp=WOS_CPL
ID情報
  • DOI : 10.1063/1.4975697
  • ISSN : 2158-3226
  • Web of Science ID : WOS:000402797100220

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