論文

査読有り
2019年3月16日

Flow visualization of heavy oil in a packed bed using real-time neutron radiography

Chemical Engineering Science
  • Eita Shoji
  • ,
  • Koshiro Yamagiwa
  • ,
  • Masaki Kubo
  • ,
  • Takao Tsukada
  • ,
  • Seiichi Takami
  • ,
  • Katsumi Sugimoto
  • ,
  • Daisuke Ito
  • ,
  • Yasushi Saito
  • ,
  • Shogo Teratani

196
開始ページ
425
終了ページ
432
記述言語
英語
掲載種別
研究論文(学術雑誌)
DOI
10.1016/j.ces.2018.11.021

Neutron radiography can visualize heavy oil flows in metallic reactors used to upgrade heavy oils. Thus, we visualized heavy oil flows in a packed bed using real-time neutron radiography to support its capability and to offer basic experimental data necessary for verification and validation of numerical simulations. Atmospheric residue was used as the heavy oil sample and heavy oil and N 2 gas were concurrently supplied into a packed bed from above a reactor simulating a trickle bed reactor. Reactor temperatures were set at either 100°C or 250°C to change heavy oil viscosity. The heavy oil flow rate was kept constant at 2.5 mL/min and the N 2 gas flow rate was set at either 1 L/min or 3 L/min at 25°C. A series of neutron radiography experiments was conducted at the B-4 neutron imaging facility in the Kyoto University Research Reactor (KUR) with a thermal neutron flux of 5 × 10 7 n/cm 2 ⋅s. We performed image processing for the neutron radiographs to calculate neutron beam attenuation and clarify flow behavior. Visualization results show differences in flow behavior depending on operating factors. Temperature had a particularly substantial effect on flow behavior because heavy oil viscosity depends strongly on temperature. The flows also showed different behaviors for 1 mm and 3 mm packed particle sizes because the void ratios in the packed bed, which were preliminarily observed by X-ray computational tomography (CT), change with particle size. Channeling flow was observed with 3 mm particles and a temperature of 250°C. Furthermore, this work suggests that neutron radiography can be used to investigate heavy oil flows in metallic reactors.

リンク情報
DOI
https://doi.org/10.1016/j.ces.2018.11.021
Scopus
https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=85056653738&origin=inward
Scopus Citedby
https://www.scopus.com/inward/citedby.uri?partnerID=HzOxMe3b&scp=85056653738&origin=inward
ID情報
  • DOI : 10.1016/j.ces.2018.11.021
  • ISSN : 0009-2509
  • SCOPUS ID : 85056653738

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