2000年
Determination of major metals in arctic snow by inductively coupled plasma mass spectrometry with cold plasma and microconcentric nebulization techniques
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY
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- 巻
- 76
- 号
- 2
- 開始ページ
- 135
- 終了ページ
- 144
- 記述言語
- 英語
- 掲載種別
- 研究論文(学術雑誌)
- DOI
- 10.1080/03067310008034125
- 出版者・発行元
- GORDON BREACH SCI PUBL LTD
A method was developed for the determination of K, Ca, Mg, Na, Al and Fe in Arctic snow samples by inductively coupled plasma mass spectrometry. Shield torch system under cold plasma conditions was used to overcome the spectral interferences from the plasma gas on K-39 ((ArH)-Ar-38), Ca-40 (Ar-40) and Fe-56 ((ArO)-Ar-40-O-16). Detection limits (3 sigma) were 1, 1, 2, 7, 6 and 3 ng/l for Na, Mg, Al, K, Ca and Fe, respectively. Reproducibility of measurements was better than 2% relative standard deviation (n=10) for all the elements of interest at 1.0 mu g/l level. The sample consumption was ca. 60 mu l per assay due to the use of a microconcentric nebulizer. Several Arctic snow samples were analysed and the reliability of the proposed method was confirmed by electrothermal atomic absorption spectrometry.
- リンク情報
- ID情報
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- DOI : 10.1080/03067310008034125
- ISSN : 0306-7319
- J-Global ID : 200902196113042811
- Web of Science ID : WOS:000088132100005