2010年
A facile and practical solvent-free one-pot synthesis of (Z)-4-methylene-3-selenaquinoline derivatives from o-ethynylanilines and isoselenocyanates
Synthesis
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- 巻
- 号
- 18
- 開始ページ
- 3091
- 終了ページ
- 3096
- 記述言語
- 掲載種別
- 研究論文(学術雑誌)
- DOI
- 10.1055/s-0030-1258171
Heating of o-ethynylanilines with isoselenocyanates directly resulted in the 6-exo-dig mode ring-closure reaction of the adducts to give the (Z)-2-imino-4-methylene-3-selenaquinolines in moderate to good yields. Based on this convenient, solvent-free, catalyst-free method, several 3-selenaquinoline derivatives (3,1-benzoselenazines) were easily obtained in one pot. Successful application of the microwave-assisted synthesis of these compounds was also investigated. © Georg Thieme Verlag Stuttgart - New York.
- リンク情報
- ID情報
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- DOI : 10.1055/s-0030-1258171
- ISSN : 0039-7881
- eISSN : 1437-210X
- ORCIDのPut Code : 51044820
- SCOPUS ID : 77956489743