2018年3月
Development of a pressure cell using a beta-titanium alloy for a Differential Scanning Calorimeter
Journal of Physics: Conference Series
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- 巻
- 969
- 号
- 1
- 開始ページ
- 012089
- 終了ページ
- 012089
- 記述言語
- 英語
- 掲載種別
- 研究論文(学術雑誌)
- DOI
- 10.1088/1742-6596/969/1/012089
- 出版者・発行元
- {IOP} Publishing
We have developed downsizing a piston-cylinder clamp-cell to measure a specific heat under pressure using a commercial Differential Scanning Calorimeter (Shimadzu DSC-60 plus). The downsized cell with a diameter of 6.0 mm and a height of 5.0 mm has been achieved by a simplification of the cell design and using a high-yield-strength alloy of β-Titanium (KOBELCO, KS15-5-3). The cell allows us to achieve pressures of 0.7 GPa at room temperature as our designed value. As a demonstration of the cell, we have measured the specific heat anomaly due to the first-order transition at around 357 K in Ca2RuO4. The pressure variation of the transition temperature indicates that our cell allows us to achieve pressure of ∼0.3 GPa. Moreover, we have estimated that a heat capacity of ∼0.6 mJ/K is fully possible to measure within β-Titanium cell as absolute accuracy.
- リンク情報
- ID情報
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- DOI : 10.1088/1742-6596/969/1/012089
- ISSN : 1742-6596
- ORCIDのPut Code : 95559992
- SCOPUS ID : 85046096529