論文

査読有り
2018年3月

Development of a pressure cell using a beta-titanium alloy for a Differential Scanning Calorimeter

Journal of Physics: Conference Series
  • T Eto
  • ,
  • K Akagi
  • ,
  • E Takashima
  • ,
  • A Noguchi
  • ,
  • T Sakami
  • ,
  • T Noda
  • ,
  • F Nakamura

969
1
開始ページ
012089
終了ページ
012089
記述言語
英語
掲載種別
研究論文(学術雑誌)
DOI
10.1088/1742-6596/969/1/012089
出版者・発行元
{IOP} Publishing

We have developed downsizing a piston-cylinder clamp-cell to measure a specific heat under pressure using a commercial Differential Scanning Calorimeter (Shimadzu DSC-60 plus). The downsized cell with a diameter of 6.0 mm and a height of 5.0 mm has been achieved by a simplification of the cell design and using a high-yield-strength alloy of β-Titanium (KOBELCO, KS15-5-3). The cell allows us to achieve pressures of 0.7 GPa at room temperature as our designed value. As a demonstration of the cell, we have measured the specific heat anomaly due to the first-order transition at around 357 K in Ca2RuO4. The pressure variation of the transition temperature indicates that our cell allows us to achieve pressure of ∼0.3 GPa. Moreover, we have estimated that a heat capacity of ∼0.6 mJ/K is fully possible to measure within β-Titanium cell as absolute accuracy.

リンク情報
DOI
https://doi.org/10.1088/1742-6596/969/1/012089
URL
https://iopscience.iop.org/article/10.1088/1742-6596/969/1/012089/meta
ID情報
  • DOI : 10.1088/1742-6596/969/1/012089
  • ISSN : 1742-6596
  • ORCIDのPut Code : 95559992
  • SCOPUS ID : 85046096529

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