2007年10月
Electrochemical O-glycosylation using thioglycosides as glycosyl donors in the presence of a catalytic amount of sodium trifluoromethanesulfonate as a supporting electrolyte
TETRAHEDRON LETTERS
- ,
- ,
- ,
- ,
- 巻
- 48
- 号
- 41
- 開始ページ
- 7383
- 終了ページ
- 7387
- 記述言語
- 英語
- 掲載種別
- 研究論文(学術雑誌)
- DOI
- 10.1016/j.tetlet.2007.08.004
- 出版者・発行元
- PERGAMON-ELSEVIER SCIENCE LTD
Electrochemical O-glycosylation of primary alcohols with O-protected thioglycosides was performed in the presence of a small amount of sodium trifluoromethansulfonate (12.5 mol % to glycosyl acceptor) as a supporting electrolyte. The reaction was successfully carried out in an undivided cell to give O-glycosides in good yields with a high electro-efficiency (ca. I F/mol) at 15 degrees C in acetonitrile. (C) 2007 Elsevier Ltd. All rights reserved.
- リンク情報
- ID情報
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- DOI : 10.1016/j.tetlet.2007.08.004
- ISSN : 0040-4039
- Web of Science ID : WOS:000249846600032