Papers

Jan 20, 2020

Anomalous size-dependent strength in micropillar compression deformation of commercial-purity aluminum single-crystals

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
  • Naoki Takata
  • ,
  • Soichiro Takeyasu
  • ,
  • Hongmei Li
  • ,
  • Asuka Suzuki
  • ,
  • Makoto Kobashi

Volume
772
Number
Language
English
Publishing type
Research paper (scientific journal)
DOI
10.1016/j.msea.2019.138710
Publisher
ELSEVIER SCIENCE SA

An anomalously reduced size-dependent strength of commercial-purity aluminum (Al) single-crystal micropillars with diameters ranging approximately from 1 to 10 mu m is reported. High-purity Al (99.99%) single-crystal micropillars exhibited an obvious size dependence of the resolved shear stress for slip. The measured shear stress resolved onto a primary slip system (tau(i)) scaled by the shear modulus (G) and the pillar diameter (d) scaled by the Burgers vector (b) showed the following correlation: tau(i)/G = 0.33(d/b)(-0.63), which agreed well with previous works. However, the commercial-purity Al samples exhibited a lower power-law exponent (0.19) for their size-dependent strength, resulting in (tau(i)/G) = 0.006(d/b)(-0.19). TEM characterization revealed the local presence of Al-Fe intermetallic precipitates surrounded by relatively high-density dislocations in annealed commercial-purity Al samples. These results indicate the relatively high-density dislocations could be responsible for the reduced size-dependent strength, which was confirmed by the remarkably reduced size dependence of their resolved shear stress by prior cold rolling. The reduced size-dependent strength can be rationalized using the stochastic model of the dislocation source length. Thus, this study provides a new insight to allow the application of the micropillar compression test to commercially produced Al alloys.

Link information
DOI
https://doi.org/10.1016/j.msea.2019.138710
Web of Science
https://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=JSTA_CEL&SrcApp=J_Gate_JST&DestLinkType=FullRecord&KeyUT=WOS:000509621500014&DestApp=WOS_CPL
ID information
  • DOI : 10.1016/j.msea.2019.138710
  • ISSN : 0921-5093
  • eISSN : 1873-4936
  • Web of Science ID : WOS:000509621500014

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